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    ASTM D3257-06(2012)

    Standard Test Methods for Aromatics in Mineral Spirits by Gas Chromatography (Withdrawn 2021)
    • 발행일 : 2012-06-01
    • 발행기관 : ASTM
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상세정보

분야 06.04 : 페인트-솔벤트; 방향성 탄화수소
적용범위

1.1 These test methods cover the determination of ethylbenzene and total eight-carbon (C8) and heavier aromatics in the concentration range from 0.1 to 30 % in mineral spirits having a distillation range from 149 to 210°C (300 to 410°F) as determined by Test Method D86. The procedures permit the identification and calculation of concentrations of aromatic components to 0.1 volume %.

1.2 It is recognized by analytical chemists that a single column gas chromatography analysis of an unknown sample is risky. In such cases, multiple and different analytical techniques must be used for absolutely positive identification, for example, several different gas chromatography columns, gas chromatography/mass spectrometer, or gas chromatography/infrared, etc. In these test methods the material is known and is clearly defined.

1.3 Oxygenated compounds, if present, may interfere and cause erroneous results. Such oxygenated compounds are not normally present in mineral spirits.

1.4 Three test methods are covered as follows:

1.4.1 Test Method A, measurement of ethylbenzene content, C8 plus higher aromatics (except ethylbenzene), and total aromatics by means of a single packed column gas chromatographic analysis.

1.4.2 Test Method B, measurement of ethylbenzene content by means of a rapid packed column gas chromatographic analysis.

1.4.3 Test Method C, measurement of ethylbenzene content, C8 plus higher aromatics (except ethylbenzene) and total aromatics by means of a capillary column gas chromatographic analysis.

1.5 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

1.6 For purposes of determining conformance of an observed or a calculated value using this test method to relevant specifications, test result(s) shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29.

1.7 For hazard information and guidance, see the supplier's Material Safety Data Sheet.

1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
국제분류(ICS)코드 87.060.30 : 용매, 첨가제 및 기타 보존재
페이지수 8
Edition 06(2012)

이력정보

No. 표준번호 표준명 발행일 상태
1 ASTM D3257-22상세보기 Standard Test Methods for Aromatics in Mineral Spirits by Gas Chromatography 2022-01-01 표준
2 ASTM D3257-06(2012)상세보기 Standard Test Methods for Aromatics in Mineral Spirits by Gas Chromatography (Withdrawn 2021) 2012-06-01 구판
3 ASTM D3257-06상세보기 Standard Test Methods for Aromatics in Mineral Spirits by Gas Chromatography 2006-04-01 구판
4 ASTM D3257-97상세보기 Standard Test Methods for Aromatics in Mineral Spirits by Gas Chromatography 2001-06-10 구판
5 ASTM D3257-01상세보기 Standard Test Methods for Aromatics in Mineral Spirits by Gas Chromatography 2001-06-10 구판
6 ASTM D3257-93e1상세보기 Standard Test Methods for Aromatics in Mineral Spirits by Gas Chromatography 구판

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